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LTC 077-2015 Former Par 3 Golf Course Update MIAMI OFFICE OF THE CITY MANAGER 20 FB37 ; NO. LTC # 077-205 v�t ci_I__ : 'L �L" 'TIER TO COMMISSION TO: Mayor Philip Levine and Members of e City Co ission FROM: Jimmy L. Morales, City Manager DATE: February 20, 2015 SUBJECT: FORMER PAR 3 GOLF COURSE PDATE The purpose of this Letter to Commission (LTC) is to provide an update on the former Par 3 golf course property. In November 2014, the City accepted fill material from the Florida Department of Transportation (FDOT) Alton Road project and the Faena project at 34 Street. The purpose was to reuse excess clean fill material generated by projects throughout the city so as to reduce the need to purchase newly mined material, which is more expensive and less sustainable. The only material accepted from FDOT was from areas of the project that did not have any environmental restrictions as determined by the FDOT Environmental Management Office. Attachment A provides the sampling results provided by the Faena for the material removed at 34 Street. While the material was determined to be clean by both sources before its delivery, the City observed potential concerns with the material and determined that independent testing was appropriate. In December 2014, City staff engaged a consultant to sample the material to confirm that the material from both locations was in fact clean fill. In January 2015, the results from this secondary evaluation were received by the City. Miami-Dade County Department of Regulatory and Economic Resources Division of Environmental Resources Management (DERM) was contacted for further guidance on these results. DERM reviewed the reports provided by the FDOT and the Faena, as well as the samples the City collected from the site and determined that additional sampling was required. The City requested assistance from DERM regarding the additional sampling and provide guidance as to the soil's re-use potential. On February 5, DERM conducted additional sampling at the site and indicated that sampling results would be available within approximately a week. Nevertheless, I directed Public Works to remove the material once the Boat Show ended and traffic would not be disrupted. On February 19, DERM provided the sample results in the form of a letter outlining their recommendations (Attachment B). Based upon the results, the City instructed a contractor to begin removal of the material from the site immediately at no cost to the City. Following the beginning of the removal activities today, DERM issued a Cease and Desist Order based upon questions regarding the disposal of the material. Shortly following the Order, DERM forwarded the February 19 letter to the Bayshore Home Owners Association. The Administration will be meeting with DERM next week to attempt to resolve their concerns so that we can continue with soil removal, proper disposal and sodding of the area. Please let me know if you have any questions or comments. i LTC-Par 3 Update February 20, 2015 Page 2 of 2 Attachments: A— Faena (Saxony West) Soil Analytical Results B— Letter from DERM dated February 19, 2015 MT/ETC/ESW/MKW F-Al.;VORK\SALL' 1)EMPLOYEE FOLDERS'�ETSY 6 HEATON\'.TC,Par 3i'Par 3 Update L T C 2.3.15.do-x Attachment® A Pace Analytical Services,Inc. ^Q q��i n�� _ ___ 3610 Park Central Blvd N Vt�A Pompano Beach,FL 33064 ( wwwpacelabs.com 954-582-4300 I. November 17, 2014 Richard Fesdijian NV5 14486 Commerce Way Hialeah, FL 33016 RE: Project: SAXONY WEST Pace Project No.: 35163711 Dear Richard Fesdijian: Enclosed are the analytical results for sample(s) received by the laboratory between November 13, 2014 and November 14, 2014. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Rossy Guima rossy.guima@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS u^< This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 1 of 25 Pace Analytical Services,Inc. _ aceAnalytical 3610 Park Central Blvd N Pompano Beach,FL 33064 wwwp4relabs.com 954-582-4300 t. CERTIFICATIONS Project: SAXONY WEST Pace Project No.: 35163711 Ormond Beach Certification IDs 8 East Tower Circle,Ormond Beach,FL 32174 Missouri Certification#:236 Alabama Certification#:41320 Montana Certification#:Cert 0074 Arizona Certification#:AZ0735 Nebraska Certification:NE-OS-28-14 Colorado Certification:FL NELAC Reciprocity Nevada Certification:FL NELAC Reciprocity Connecticut Certification#:PH-0216 New Hampshire Certification#:2958 Delaware Certification:FL NELAC Reciprocity New Jersey Certification#:FL765 Florida Certification#:E83079 New York Certification#: 11608 Georgia Certification#:955 North Carolina Environmental Certificate,#:667 Guam Certification:FL NELAC Reciprocity North Carolina Certification#: 12710 Hawaii Certification:FL NELAC Reciprocity Pennsylvania Certification#:68-00547 Illinois Certification#:200068 Puerto Rico Certification#:FLO1264 Indiana Certification:FL NELAC Reciprocity South Carolina Certification:#96042001 Kansas Certification#:E-10383 Tennessee Certification#:TN02974 Kentucky Certification#:90050 Texas Certification:FL NELAC Reciprocity Louisiana Certification#:FL NELAC Reciprocity US Virgin Islands Certification:FL NELAC Reciprocity Louisiana Environmental Certificate#:05007 Virginia Environmental Certification#:460.165 Maryland Certification:#346 Washington Certification#:C955 Massachusetts Certification#:M-FL1264 West Virginia Certification#:9962C Michigan Certification#:9911 Wisconsin Certification#:399079670 Mississippi Certification:FL NELAC Reciprocity Wyoming(EPA Region 8):FL NELAC Reciprocity REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 2 of 25 I Pace Analytical Services,Inc. aceAnalytical 3610 Park Central Blvd N Pompano Beach,FL 33064 fl www.pacelabs.com 954-582-4300 i 3 I SAMPLE SUMMARY Project: SAXONY WEST Pace Project No.: 35163711 Lab ID Sample ID Matrix Date Collected Date Received 35163711001 B-1 S-10 Solid 11/13/14 08:00 11/13/14 18:10 35163711002 Stockpile Sample Solid 11/13/14 08:00 11/14/14 08:38 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 3 of 25 Pace Analytical Services,Inc. Q �7 ��+ f® 3610 Park Central Blvd N ac��AI alyti a Pompano Beach,FL 33064 i www.pawlabs.wm 954-582-4300 I SAMPLE ANALYTE COUNT Project: SAXONY WEST Pace Project No.: 35163711 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 35163711001 B-1 S-10 EPA 8081 JLG 22 PASI-O EPA 8141 WFH 20 PASI-O EPA 8151 JTJ 11 PASI-O FL-PRO JGW 3 PASI-O EPA 6010 CKJ 2 PASI-O EPA 7471 CKJ 1 PASI-O ASTM D2974-87 AJK 1 PASI-O 35163711002 Stockpile Sample EPA 8081 JLG 22 PASI-O EPA 8141 WFH 20 PASI-O EPA 8151 JTJ 11 PASI-O FL-PRO JGW 3 PASI-O EPA 6010 CKJ 2 PASI-O EPA 7471 CKJ 1 PASI-O ASTM D2974-87 AJK 1 PASI-O REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 4 of 25 Pace Analytical Services,Inc. N. ® 3610 Park Central Blvd N axAnalytical Pompano Beach,FL 33064 www.pnelabs.com 954-582-4300 I � I. ANALYTICAL RESULTS Project: SAXONY WEST Pace Project No.: 35163711 Sample: B-1 S-10 Lab ID: 35163711001 Collected: 11/13/14 08:00 Received: 11/13/14 18:10 Matrix: Solid Results reported on a"dry-weight"basis Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method:EPA 8081 Preparation Method:EPA 3546 Aldrin 0.000069U mg/kg 0.0020 0.000069 1 11/14/14.16:15 . 11/15/14 00:56 309-00-2. alpha-BHC 0.000082U mg/kg 0.0020 0.000082 1 11/14/14 16:15 11/15/14 00:56 319-84-6 beta-BHC 0.000092U mg/kg 0.0020 0.000092 1 11/14/14 16:15 11/15/14 00:56 319-85-7 delta-BHC 0.00010U mg/kg 0.0020 0.00010 1 11/14/14 16:15 11/15/14 00:56 319-86-8 gamma-BHC(Lindane) 0.000180 mg/kg 0.0020 0.00018 1 11/14/14 16:15 11/15/14 00:56 58-89-9 Chlordane(Technical) 0.019U mg/kg 0.020 0.019 1 11/14/14 16:15 11/15/14 00:56 57-74-9 4,4'-DDD 0.000160 mg/kg 0.0020 0.00016 1 11/14/14 16:15 11/15/14 00:56 72-54-8 4,4'-DDE 0.00131 mg/kg 0.0020 0.000073 1 11/14/14 16:15 11/15/14 00:56 72-55-9 4,4'-DDT 0.000451 mg/kg 0.0020 0.00011 1 11/14/14 16:15 11/15/14 00:56 50-29-3 Dieldrin 0.000211 mg/kg 0.0020 0.000048 1 11/14/14 16:15 11/15/14 00:56 60-57-1 Endosulfan 1 0.000030U mg/kg 0.0020 0.000030 1 11/14/14 16:15 11/15/14 00:56 959-98-8 Endosulfan II 0.000171 mg/kg 0.0020 0.000068 1 11/14/14 16:15 11/15/14 00:56 33213-65-9 Endosulfan sulfate 0.000051U mg/kg 0.0020 0.000051 1 11/14/14 16:15 11/15/14 00:56 1031-07-8 Endrin 0.0000620 mg/kg 0.0020 0.000062 1 11/14/14 16:15 11/15/14 00:56 72-20-8 Endrin aldehyde 0.0000790 mg/kg 0.0039 0.000079 1 11/14/14 16:15 11/15/14 00:56 7421-93-4 End6n ketone 0.000095U mg/kg 0.0020 0.000095 1 11/14/14 16:15 11/15/14 00:56 53494-70-5 Heptachlor 0.0000470 mg/kg 0.0020 0.000047 1 11/14/14 16:15 11/15/14 00:56 76-44-8 Heptachlor epoxide 0.000130 mg/kg 0.0020 0.00013 1 11/14/14 16:15 11/15/14 00:56 1024-57-3 Methoxychlor 0.00130 mg/kg 0.0020 0.0013 1 11/14/14 16:15 11/15/14 00:56 72-43-5 Toxaphene 0.0088U mg/kg 0.020 0.0088 1 11/14/14 16:15 11/15/14 00:56 8001-35-2 Surrogates Tetrachloro-m-xylene(S) 86 % 53-130 1 11/14/14 16:15 11/15/14 00:56 877-09-8 Decachlorobiphenyl(S) 68 % 10-130 1 11/14/14 16:15 11/15/14 00:56 2051-24-3 8141 O/P Pesticides Microwave Analytical Method:EPA 8141 Preparation Method:EPA 3546 Atrazine 0.00920 mg/kg 0.059 0.0092 1 11/13/14 23:00 11/14/14 11:46 1912-24-9 Azinphos,methyl(Guthion) 0.00460 mg/kg 0.020 0.0046 1 11/13/14 23:00 11/14/14 11:46 86-50-0 Bromacil 0.0 mg/kg 1 11/13/14 23:00 11/14/14 11:46 314-40-9 N2 Carbophenothion(Trithion) 0.0049U mg/kg 0.020 0.0049 1 11/13/14 23:00 11/14/14 11:46 786-19-6 Chlorpyrifos 0.0035U mg/kg 0.020 0.0035 1 11/13/14 23:00 11/14/14 11:46 2921-88-2 Coumaphos 0.013U mg/kg 0.020 0.013 1 11/13/14 23:00 11/14/14 11:46 56-72-4 Diazinon 0.0038U mg/kg 0.020 0.0038 1 11/13/14 23:00 11/14/14 11:46 333-41-5 Dichlorvos 0.0047U mg/kg 0.020 0.0047 1 11/13/14 23:00 11/14/14 11:46 62-73-7 Dimethoate 0.0038U mg/kg 0.020 0.0038 1 11/13/14 23:00 11/14/14 11:46 60-51-5 Disulfoton 0.0037U mg/kg 0.020 0.0037 1 11/13/14 23:00 11/14/14 11:46 298-04-4 Ethion 0.0042U mg/kg 0.020 0.0042 1 11/13/14 23:00 11/14/14 11:46 563-12-2 Famphur 0.00440 mg/kg 0.020 0.0044 1 11/13/14 23:00 11/14/14 11:46 52-85-7 Malathion 0.0037U mg/kg 0.020 0.0037 1 11/13/14 23:00 11/14/14 11:46 121-75-5 Methyl parathion 0.0053U mg/kg 0.020 0.0053 1 11/13/14 23:00 11/14/14 11:46 298-00-0 Mevinphos 0.00350 mg/kg 0.020 0.0035 1 11/13/14 23:00 11/14/14 11:46 7786-34-7 Monocrotophos 0.0085U mg/kg 0.039 0.0085 1 11/13/14 23:00 11/14/14 11:46 919-44-8 L3 Parathion(Ethyl parathion) 0.00770 mg/kg 0.039 0.0077 1 11/13/14 23:00 11/14/14 11:46 56-38-2 Phorate 0.00680 mg/kg 0.039 0.0068 1 11/13/14 23:00 11/14/14 11:46 298-02-2 Phosmet 0.0086U mg/kg 0.020 0.0086 1 11/13/14 23:00 11/14/14 11:46 732-11-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 5 of 25 Pace Analytical Services,Inc. ® 3610 Park Central Blvd N ace Analytical Pompano Beach,FL 33064 www.pacelabs.com 954-582-4300 i i ANALYTICAL RESULTS Project: SAXONY WEST Pace Project No.: 35163711 Sample: B-1 S-10 Lab ID: 35163711001 Collected: 11/13/14 08:00 Received: 11/13/14 18:10 Matrix: Solid Results reported on a"dry-weight"basis Parameters Results Units PQL MDL- DF Prepared Analyzed CAS No. Qual 8141 O/P Pesticides Microwave Analytical Method:EPA 8141 Preparation Method:EPA 3546 Surrogates 4-Chloro3nitrobenzotrifluodde 52 % 28.9- 1 11/13/1423:00 11/14/1411:46 136.7 8151 Chlorinated Herbicides Analytical Method:EPA 8151 Preparation Method:EPA 8151 Bentazon 0.0023U mg/kg 0.0037 0.0023 1 11/14/14 08:00 11/14/14 19:28 25057-89-0 2,4-D 0.00890 mg/kg 0.037 0.0089 1 11/14/14 08:00 11/14/14 19:28 94-75-7 Dalapon 0.00720 mg/kg 0.036 0.0072 1 11/14/14 08:00 11/14/14 19:28 75-99-0 2,4-DB 0.020U mg/kg 0.074 0.020 1 11/14/14 08:00 11/14/14 19:28 94-82-6 Dicamba 0.00150 mg/kg 0.0037 0.0015 1 11/14/14 08:00 11/14/14 19:28 1918-00-9 Dinoseb 0.0018U mg/kg 0.0074 0.0018 1 11/14/14 08:00 11/14/14 19:28 88-85-7 Pentachlorophenol 0.0015 mg/kg 0.0011 0.00096 1 11/14/14 08:00 11/14/14 19:28 87-86-5 Picloram 0.00063U mg/kg 0.0037 0.00063 1 11/14/14 08:00 11/14/14 19:28 1918-02-1 2,4,5-T 0.0013U mg/kg 0.0075 0.0013 1 11/14/14 08:00 11/14/14 19:28 93-76-5 2,4,5-TP(Silvex) 0.000940 mg/kg 0.0075 0.00094 1 11/14/14 08:00 11/14/14 19:28 93-72-1 Surrogates 2,4-DCAA(S) 84 % 66-130 1 11/14/14 08:00 11/14/14 19:28 19719-28-9 FL-PRO Soil Microwave Analytical Method:FL-PRO Preparation Method:EPA 3546 Petroleum Range Organics 31.3 mg/kg 4.7 3.0 1 11/14/14 02:00 11/14/14 14:47 Surrogates o-Terphenyl(S) 106 % 62-109 1 11/14/14 02:00 11/14/14 14:47 84-15-1 N-Pentatriacontane(S) 106 % 42-159 1 11/14/14 02:00 11/14/14 14:47 630-07-09 6010 MET ICP Analytical Method:EPA 6010 Preparation Method:EPA 3050 Arsenic 6.7 mg/kg 0.58 0.29 1 11/16/14 05:55 11/17/14 13:48 7440-38-2 Lead 0.69 mg/kg 0.58 0.29 1 11/16/14 05:55 11/17/14 13:48 7439-92-1 7471 Mercury Analytical Method:EPA 7471 Preparation Method:EPA 7471 Mercury 0.0062 mg/kg 0.0048 0.0024 1 11/17/1410:29 11/17/1415:41 7439-97-6 Percent Moisture Analytical Method:ASTM D2974-87 Percent Moisture 15.4 % 0.10 0.10 1 11/17/14 07:27 J(D6) REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 6 of 25 Pace Analytical Services,Inc. 3610 Park Central Blvd N aceAnalXical Pompano Beach,FL 33064 www.pacelabs.com 954-582-4300 i. ANALYTICAL RESULTS Project: SAXONY WEST Pace Project No.: 35163711 Sample: Stockpile Sample Lab ID: 35163711002 Collected: 11/13/14 08:00 Received: 11/14/14 08:38 Matrix: Solid Results reported on a"dry-weight'basis Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method:EPA 8081 Preparation Method:EPA 3546 Aldrin 0.000063U mg/kg 0.0019 0.000063 1 11/14/14 16:15 11/15/14 23:37 309-00-2 alpha-BHC 0.0000751.11 mg/kg 0.0019 0.000075 1 11/14/14 16:15 11/15/14 23:37 319-84-6 beta-BHC 0.000084U mg/kg 0.0019 0.000084 1 11/14/14 16:15 11/15/14 23:37 319-85-7 delta-BHC 0.0000950 mg/kg 0.0019 0.000095 1 11/14/14 16:15 11/15/14 23:37 319-86-8 gamma-BHC(Lindane) 0.000160 mg/kg 0.0019 0.00016 1 11/14/14 16:15 11/15/14 23:37 58-89-9 Chlordane(Technical) 0.017U mg/kg 0.019 0.017 1 11/14/14 16:15 11/15/14 23:37 57-74-9 4,4'-DDD 0.00014U.mg/kg 0.0019 0.00014 1 11/14/14 16:15 11/15/14 23:37 72-54-8 4,4'-DDE 0.000841 mg/kg 0.0019 0.000067 1 11/14/14 16:15 11/15/14 23:37. 72-55-9 4,4'-DDT 0.000281 mg/kg 0.0019 0.00010 1 11/14/14 16:15 11/15/14 23:37 50-29-3 Dieldrin 0.0000701 mg/kg 0.0019 0.000044 1 11/14/14 16:15 11/15/14 23:37 60-57-1 Endosulfan I 0.000027U mg/kg 0.0019 0.000027 1 11/14/14 16:15 11/15/14 23:37 959-98-8 Endosulfan II 0.0000620 mg/kg 0.0019 0.000062 1 11/14/14 16:15 11/15/14 23:37 33213-65-9 Endosulfan sulfate 0.000047U mg/kg 0.0019 0.000047 1 11/14/14 16:15 11/15/14 23:37 1031-07-8 Endrin 0.000057U mg/kg 0.0019 0.000057 1 11/14/14 16:15 11/15/14 23:37 72-20-8 Endrin aldehyde 0.000072U mg/kg 0.0036 0.000072 1 11/14/14 16:15 11/15/14 23:37 7421-93-4 Endrin ketone 0.000087U mg/kg 0.0019 0.000087 1 11/14/14 16:15 11/15/14 23:37 53494-70-5 Heptachlor 0.000043U mg/kg 0.0019 0.000043 1 11/14/14 16:15 11/15/14 23:37 76-44-8 Heptachlor epoxide 0.00012U mg/kg 0.0019 0.00012 1 11/14/14 16:15 11/15/14 23:37 1024-57-3 Methoxychlor 0.00110 mg/kg 0.0019 0.0011 1 11/14/14 16:15 11/15/14 23:37 72-43-5 Toxaphene 0.0080U mg/kg 0.019 0.0080 1 11/14/14 16:15 11/15/14 23:37 8001-35-2 Surrogates Tetrachloro-m-xylene(S) 89 % 53-130 1 11/14/14 16:15 11/15/14 23:37 877-09-8 Decachlorobiphenyl(S) 85 % 10-130 1 11/14/14 16:15 11/15/14 23:37 2051-24-3 8141 O/P Pesticides Microwave Analytical Method:EPA 8141 Preparation Method:EPA 3546 Atrazine 0.017U mg/kg 0.11 0.017 1 11/14/14 23:00 11/17/14 11:12 1912-24-9 Azinphos,methyl(Guthion) 0.0085U mg/kg 0.036 0.0085 1 11/14/14 23:00 11/17/14 11:12 86-50-0 Bromacil 0.0 mg/kg 1 11/14/14 23:00 11/17/14 11:12 314-40-9 N2 Carbophenothion(Trithion) 0.0089U mg/kg 0.036 0.0089 1 11/14/14 23:00 11/17/14 11:12 786-19-6 Chlorpyrifos 0.0064U mg/kg 0.036 0.0064 1 11/14/14 23:00 11/17/14 1112 2921-88-2 Coumaphos 0.024U mg/kg 0.036 0.024 1 11/14/14 23:00 11/17/14 11:12 56-72-4 Diazinon 0.0069U mg/kg 0.036 0.0069 1 11/14/14 23:00 11/17/14 11:12 333-41-5 Dichlorvos 0.00850 mg/kg 0.036 0.0085 1 11/14/14 23:00 11/17/14 11:12 62-73-7 Dimethoate 0.0069U mg/kg 0.036 0.0069 1 11/14/14 23:00 11/17/14 11:12 60-51-5 Disulfoton 0.0068U mg/kg 0.036 0.0068 1 11/14/14 23:00 11/17/14 11:12 298-04-4 Ethion 0.0077U mg/kg 0.036 0.0077 1 11/14/14 23:00 11/17/14 11:12 563-12-2 Famphur 0.00800 mg/kg 0.036 0.0080 1 11/14/14 23:00 11/17/14 11:12 52-85-7 Malathion 0.0068U mg/kg 0.036 0.0068 1 11/14/14 23:00 11/17/14 11:12 121-75-5 Methyl parathion 0.00980 mg/kg 0.036 0.0098 1 11/14/14 23:00 11/17/14 11:12 298-00-0 Mevinphos 0.0064U mg/kg 0.036 0.0064 1 11/14/14 23:00 11/17/14 11:12 7786-34-7 Monocrotophos 0.016U mg/kg 0.072 0.016 1 11/14/14 23:00 11/17/14 11:12 919-44-8 Parathion(Ethyl parathion) 0.014U mg/kg 0.072 0.014 1 11/14/14 23:00 11/17/14 11:12 56-38-2 Phorate 0.012U mg/kg 0.072 0.012 1 11/14/14 23:00 11/17/14 11:12 298-02-2 Phosmet 0.0160 mg/kg 0.036 0.016 1 11/14/14 23:00 11/17/14 11:12 732-11-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 7 of 25 Pace Analytical Services,Inc. ® 3610 Park Central Blvd N ;aneAnalytical Pompano Beach,FL 33064 wwwpace/aos.com 954-582-4300 i'. ANALYTICAL RESULTS Project: SAXONY WEST Pace Project No.: 35163711 Sample: Stockpile Sample Lab ID: 35163711002 Collected: 11/13/14 08:00 Received: 11/14/14 08:38 Matrix: Solid Results reported on a"dry-weight"basis Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual 8141 O/P Pesticides Microwave Analytical Method:EPA 8141 Preparation Method:EPA 3546 Surrogates 4-Chloro3nitrobenzotrifluodde 56 % 28.9- 1 11/14/1423:00 11/17/1411:12 136.7 8151 Chlorinated Herbicides Analytical Method:EPA 8151 Preparation Method:EPA 8151 Bentazon 0.0021U mg/kg 0.0034 0.0021 1 11/14/14 08:00 11/14/14 19:58 25057-89-0 2,4-D 0.0082U mg/kg 0.034 0.0082 1 11/14/14 08:00 11/14/14 19:58 94-75-7 Dalapon 0.0066U mg/kg 0.033 0.0066 1 11/14/14 08:00 11/14/14 19:58 75-99-0 2,4-DB 0.0181.1 mg/kg 0.068 0.018 1 11/14/14 08:00 11/14/14 19:58 94-82-6 Dicamba 0.00141.11 mg/kg 0.0034 0.0014 1 11/14/14 08:00 11/14/14 19:58 1918-00-9 Dinoseb 0.00161.1 mg/kg 0.0068 0.0016 1 11/14/14 08:00 11/14/14 19:58 88-85-7 Pentachlorophenol 0.00088U mg/kg 0.0010 0.00088 1 11/14/14 08:00 11/14/14 1.9:58 87-86-5 Picloram 0.00058U mg/kg 0.0034 0.00058 1 11/14/14 08:00 11/14/14 19:58 1918-02-1 2,4,5-T 0.0012U mg/kg 0.0068 0.0012 1 11/14/14 08:00 11/14/14 19:58 93-76-5 2,4,5-TP.(Silvex) 0.00086U mg/kg 0.0069 0.00086 1 11/14/14 08:00 11/14/14 19:58 93-72-1 Surrogates, 2,4-DCAA(S) 85 % 66-130 1 11/14/14 08:00 11/14/14 19:58 19719-28-9 FL-PRO Soil Microwave Analytical Method:FL-PRO Preparation Method:EPA 3546 Petroleum Range Organics 29.3 mg/kg 11.0 7.0 1 11/14/14 17:30 11/15/14 10:39 Surrogates o-Terphenyl(S) 89 % 62-109 1 11/14/14 17:30 11/15/14 10:39 84-15-1 N-Pentatriacontane(S) 86 % 42-159 1 11/14/14 17:30 11/15/14 10:39 630-07-09 6010 MET ICP Analytical Method:EPA 6010 Preparation Method:EPA 3050 Arsenic 5.7 mg/kg 0.53 0.26 1 11/16/14 05:55 11/17/14 13:53 7440-38-2 Lead 0.291 mg/kg 0.53 0.26 1 11/16/14 05:55 11/17/14 13:53 7439-92-1 7471 Mercury Analytical Method:.EPA 7471 Preparation Method:EPA 7471 Mercury 0.0031 1 mg/kg 0.0044 0.0022 1 11/17/1410:29 11/17/1415:45 7439-97-6 Percent Moisture Analytical Method:ASTM D2974-87 Percent Moisture 8.0 % 0.10 0.10 1 11/17/14 07:28 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 8 of 25 Pace Analytical Services,Inc. �' 3610 Park Central Blvd N aci Al IaI fitraI Pompano Beach,FL 33064 www.pacelabs.com 954-582-4300 1. QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: MERP/5098 Analysis Method: EPA 7471 QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury Associated Lab Samples: 35163711001,35163711002 METHOD BLANK: 1058875 Matrix: Solid Associated Lab Samples: 35163711001,35163711002 Blank Reporting Parameter Units. Result Limit Analyzed Qualifiers Mercury mg/kg 0.0020U 0.0041 11/17/1415:37 LABORATORY CONTROL SAMPLE: 1058876 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Mercury mg/kg .08 0.078 97 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1058877 1058878 MS MSD 35163908006 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual Mercury mg/kg 0.068 .092 .088 0.14 0.14 73 80 80-120 3 20 J(M1) I Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 9 of 25 I Pace Analytical Services,Inc. ® 3610 Park Central Blvd N aceAnalytical Pompano Beach,FL 33064 l wwwpacelabs.com 954-582-4300 i. QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: MPRP/21509 Analysis Method: EPA 6010 QC Batch Method: EPA 3050 Analysis Description: 6010 MET Solid Associated Lab Samples: 35163711001,35163711002 METHOD BLANK: 1058523 Matrix: Solid Associated Lab Samples: 35163711001,35163711002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic mg/kg 0.25U 0.50 11/17/1412:17 Lead mg/kg 0.25U 0.50 11/17/1412:17 LABORATORY CONTROL SAMPLE: 1058524 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Arsenic mg/kg 12.5 12.1 97 80-120 Lead mg/kg 12.5 12.9 .103 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1058525 1058526 MS . MSD 35162667002 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual Arsenic mg/kg 5.4 81.7 79.8 84.6 81.6 97 95 75-125 4 20 Lead mg/kg 38.1 81.7 79.8 131 123 113 106 75-125 6 20 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 10 of 25 Pace Analytical Services,Inc. ® 3610 Park Central Blvd N aneAnalytical Pompano Beach,FL 33064 www.pacelabs.com 954-582-4300 j s. QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: OEXT/19690 Analysis Method: EPA 8081 QC Batch Method: EPA 3546 Analysis Description: 8081 GCS Pesticides Associated Lab Samples: 35163711001,35163711002 METHOD BLANK: 1057316 Matrix: Solid Associated Lab Samples: 35163711001,35163711002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 4,4'-DDD mg/kg 0.00013U 0.0017 11/15/1417:21 4,4'-DDE mg/kg 0.000061U 0.0017 11/15/1417:21 4,4'-DDT mg/kg 0.000096U 0.0017 11/15/1417:21 Aldrin mg/kg 0.000058U 0.0017 11/15/1417:21 alpha-BHC mg/kg 0.000069U 0.0017 11/15/1417:21 beta-BHC mg/kg 0.000077U 0.0017 11/15/1417:21 Chlordane(Technical) mg/kg 0.016U 0.017 11/15/14 17:21 delta-BHC mg/kg 0.000087U 0.0017 11/15/1417:21 Dieldrin mg/kg 0.000040U 0.0017 11/15/1417:21 Endosulfan I mg/kg 0.000025U 0.0017 11/15/14 17:21 Endosulfan II mg/kg 0.000057U 0.0017 11/15/14 17:21 Endosulfan sulfate mg/kg 0.000043U 0.0017 11/15/14 17:21 Endrin mg/kg 0.000052U' 0.0017 11/15/14 17:21 Endrin aldehyde mg/kg 0.000066U 0.0033 11/15/14 17:21 Endrin ketone mg/kg 0.000080U 0.0017 11/15/14 17:21 gamma-BHC(Lindane) mg/kg 0.00015U 0.0017 11/15/14 17:21 Heptachlor mg/kg 0.000039U 0.0017 11/15/1417:21 Heptachlor epoxide mg/kg 0.000111U 0.0017 11/15/14 17:21 Methoxychlor mg/kg 0.0010U 0.0017 11/15/1417:21 Toxaphene mg/kg 0.0073U 0.017 11/15/1417:21 Decachlorobiphenyl(S) % 93 10-130 11/15/14 17:21 Tetrachloro-m-xylene(S) % 87 53-130 11/15/14 17:21 LABORATORY CONTROL SAMPLE: 1057317 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 4,4'-DDD mg/kg 017 0.017 103 64-132 4,4'-DDE mg/kg .017 0.017 105 58-138 4,4'-DDT mg/kg .017 0.016 97 65-130 Aldrin mg/kg .017 0.016 98 64-130 alpha-BHC mg/kg .017 0.016 99 67-130 beta-BHC mg/kg .017 0.015 91 .67-130 delta-BHC mg/kg .017 0.014 87 50-130 Dieldrin mg/kg .017 0.016 99 65-130 Endosulfan I mg/kg .017 0.018 106 67-130 Endosulfan II mg/kg .017 0.017 103 66-130 Endosulfan sulfate mg/kg .017 0.017 104 61-134 Endrin mg/kg .017 0.017 103 65-132 Endrin aldehyde mg/kg .017 0.015 88 53-133 Endrin ketone mg/kg .017 0.017 103 64-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 11 of 25 i Pace Analytical Services,Inc. ® 3610 Park Central Blvd N aceAnalytical Pompano Beach,FL 33064 www.pacetabs.com 954-582-4300 t QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 LABORATORY CONTROL SAMPLE: 1057317 Spike LCS LCS %Rec Parameter Units Cone. Result %Rec Limits Qualifiers gamma-BHC(Lindane) mg/kg .017 0.016 97 65-131 Heptachlor mg/kg .017 0.016 99 65-130 Heptachlor epoxide mg/kg .017 0.016 96 66-130 Methoxychlor mg/kg .017 0.017 101 58-144 Decachlorobiphenyl(S) % 60 10-130 Tetrachloro-m-xylene(S) % 54 53-130 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1057645 1057646 MS MSD 35163393027 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qual 4,4'=DDD mg/kg 0.14U .018 .018 0.020 0.012 111 69 64-132 47 40 J(R1) ug/kg 4,4'-DDE mg/kg 0.065U .018 .018 0.020 0.013 112 72 58-138 43 40 J(R1) ug/kg 4,4'-DDT mg/kg 0.10U .018 .018 0.017 0.011 97 61 65-130 45 40 J(M1), ug/kg J(R1) Aldrin mg/kg 0.231 .018 .018 0.015 0.011 85 60 64-130 33 40 J(M1) ug/kg alpha-BHC mg/kg 0.074U .018 .018 0.015 0.011 83 59 67-130 34 40 J(M1) ug/kg beta-BHC mg/kg 0.11 1 .018 .018 0.014 0.010 78 56 67-130 33 40 J(M1) ug/kg delta-BHC mg/kg 0.093U .018 .018 0.013 0.0083 72 47 50-1.30 43 40 J(M1), ug/kg J(R1) Dieldrin mg/kg 7.0 ug/kg .018 .018 0.025 0.016 101 51 65-130 43 40 J(M1), J(R1) Endosulfan I mg/kg 0.027U .018 .018 0.020 0.014 114 78 67-130 38 40 ug/kg Endosulfan II mg/kg 0.061 U .018 .018 0.020 0.016 110 90 66-130 20 40 ug/kg Endosulfan sulfate mg/kg 0.046U .018 .018 0.015 0.0098 86 55 61-134 44 40 J(M1), ug/kg J(R1) Endrin mg/kg 0.0561-1 .018 .018 0.018 0.012 101 66 65-132 42 40 J(R1) ug/kg Endrin aldehyde mg/kg 0.070U .018 .018 0.023 0.014 128 78 53-133 49 40 J(R1) ug/kg Endrin ketone mg/kg 0.085U '.018 .018 0.015 0.0097 85 54 64-130 44 40 J(M1), ug/kg J(R1) gamma-BHC(Lindane) mg/kg 0.16U .018 .018 0.014 0.010 81 56 65-131 36 40 J(M1) ug/kg Heptachlor mg/kg 0.042U .018 .018 0.015 0.011 85 62 65-130 32 40 J(M1) ug/kg Heptachlor epoxide mg/kg 1.8 1 ug/kg .018 .018 0.017 0.012 84 55 66-130 37 40 J(M1) Methoxychlor mg/kg 1.3 1 ug/kg .018 .018 0.018 0.012 95 62 58-144 39 40 Decachlorobiphenyl(S) % 79 53 10-130 Tetrachloro-m-xylene(S) % 82 65 53-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 12 of 25 Pace Analytical Services,Inc. aceAnal Kcal 3610 Park Central Blvd N .„ Pompano Beach,FL 33064 www.pacelabs.com 954-582-4300 QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: OEXT/19664 Analysis Method: EPA 8141 QC Batch Method: EPA 3546 Analysis Description: 8141 Organophos Pests in soil Associated Lab Samples: 35163711001 METHOD BLANK: 1055345 Matrix: Solid Associated Lab Samples: 35163711001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Atrazine mg/kg 0.0078U 0.050 11/13/1411:39 Azinphos,methyl(Guthion) mg/kg 0.0039U 0.017 11/13/14 11:39 Bromacil mg/kg 0.0 11/13/1411:39 N2 Carbophenothion(Trithion) mg/kg 0.0041U 0.017 11/13/14 11:39 Chlorpyrifos mg/kg 0.0030U 0.017 11/13/1411:39 Coumaphos mg%kg 0.011U 0.017 11/13/14 11:39 Diazinon mg/kg 0.0032U 0.017 11/13/1411:39 Dichlorvos mg/kg 0.0040U 0.017 11/13/1411:39 Dimethoate mg/kg 0.0032U 0.017 11/13/1411:39 Disulfoton mg/kg 0.0031 U 0.017 11/13/14 11:39 Ethion mg/kg 0.0036U 0.017 11/13/1411:39 Famphur mg/kg 0.0037U 0.017 11/13/1411:39 Malathion mg/kg 0.0031U 0.017 11/13/1411:39 Methyl parathion mg/kg 0.0045U 0.017 11/13/14 11:39 Mevinphos mg/kg 0.0030U 0.017 11/13/1411:39 Monocrotophos mg/kg 0.0072U 0.033 11/13/1411:39 Parathion(Ethyl parathion) mg/kg 0.0065U 0.033 11/13/14 11:39 Phorate mg/kg 0.0058U 0.033 11/13/1411:39 Phosmet mg/kg 0.0072U 0.017 11/13/1411:39 4-Chloro3nitrobenzotnfluonde % 72 28.9-136.7 11/13/1411:39 LABORATORY CONTROL SAMPLE: 1055346 Spike LCS. LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Atrazine mg/kg 2 0.22 110 58-130 Azinphos,methyl(Guthion) mg/kg .067 0.081 121 47-143 Bromacil mg/kg .13 0.0 0 N2 Carbophenothion(Trithion) mg/kg .067 0.071 107 53-130 Chlorpyrifos mg/kg .067 0.063 95 60-130 Coumaphos mg/kg .067 0.070 105 50-130 Diazinon mg/kg .067 0.068 102 57-130 Dichlorvos mg/kg .067. 0.056 84 51-153 Dimethoate mg/kg .067 0.087 131 42-144 Disulfoton mg/kg .067 0.067 100 57-130 Ethion mg/kg .067 0.061 92 57-130 Famphur mg/kg .067 0.078 117 59-132 Malathion mg/kg .067 0.069 104 47-160 Methyl parathion mg/kg .067 0.063 94 57-130 Mevinphos mg/kg .067 0.060 90 50-148 Monocrotophos mg/kg .13 0.20 147 41-133 J(1-0) Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, - Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 13 of 25 Pace Analytical Services,Inc. ® 3610 Park Central Blvd N aceAnalyfical Pompano Beach,FL 33064 I www.paeelabs.com 954-582-4300 QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 LABORATORY CONTROL SAMPLE: 1055346 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Parathion(Ethyl parathion) mg/kg .13 0.15 112 54-130 Phorate mg/kg .13 0.13 95 48-130 Phosmet mg/kg .067 0.080 120 52-136. 4-Chloro3nitrobenzotrifluoride % 75 28.9-136.7 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1055619 1055620 MS MSD 35163214001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual Atrazine mg/kg 0.010U .26 .26 0.28 0.25 110 99 32-130 10 40 Azinphos,methyl(Guthion) mg/kg 0.0050U .086 .086 0.10 0.089 121 105 10-164 14 40 Bromacil mg/kg 0.0 .17 .17 0.0 0.0 0 0 N2 Carbophenothion(Trithion) mg/kg 0.0053U .086 .086 0.093 0.082 109 97 35-138 12 40 Chlorpyrifos mg/kg 0.0038U .086 .086 0.082 0.074 97 87 55-130 10 40 Coumaphos mg/kg 0.014U .086 .086 0.096 0.082 .113 97 41-130 15 40 Diazinon mg/kg 0.0041 U .086 .086 0.088 0.079 103 93 57-130 11 40 Dichlorvos mg/kg 0.0051 U . 086 .086 0.071 0.059 83 69 73-130 19 40 J(M 1) Dimethoate mg/kg 0.0041 U .086 .086 0.11 0.098 130 115 18-153 13 40 Disulfoton mg/kg 0.0040U .086 .086 0.086 0.077 101 90 47-130 11 40 Ethion mg/kg 0.0045U .086 .086 0.079 0.071 93 84 35-140 10 40 Famphur mg/kg 0.0047U .086 .086 0.10 0.093 122 109 50-130 11 40 Malathion mg/kg 0.0040U .086 .086 0.083 0.075 97 88 64-130 10 40 Methyl parathion mg/kg 0.0058U .086 .086 0.083 0.074 97 87 50-130 11 40 Mevinphos mg/kg 0.0038U .086 .086 0.075 0.066 88 78 54-134 12 40 Monocrotophos mg/kg 0.0092U .17 .17 0.28 0.23 165 134 23-131 20 40 J(MO) Parathion(Ethyl parathion) mg/kg 0.0083U .17 .17 0.20 0.18 116 104 49-130 11 40 Phorate mg/kg 0.0073U .17 .17 0.16. 0.14 96 85 38-130 12 40 Phosmet mg/kg 0.0092U .086 .086 -0.10 0.073 120 86 40-131 33 40 4- % 58 58 28.9-136 Chloro3nitrobenzotrifluoride Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 14 of 25 Pace Analytical Services,Inc. ® 3610 Park Central Blvd N a Pompano Beach,FL 33064 www.pacelabs.com 954-582-4300 i QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: OEXT/19692 Analysis Method: EPA 8141 QC Batch Method: EPA 3546 Analysis Description: 8141 Organophos Pests in soil Associated Lab Samples: 35163711002 METHOD BLANK: 1057380 Matrix: Solid Associated Lab Samples: 35163711002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Atrazine mg/kg 0.0078U 0.050 11/17/14 09:55 Azinphos,methyl(Guthion) mg/kg 0.0039U 0.017 11/17/14 09:55 Bromacil mg/kg 0.0 11/17/14 09:55 N2 Carbophenothion(Trithion) mg/kg 0.0041 U 0.017 11/17/14 09:55 Chlorpyrifos mg/kg 0.0030U 0.017 11/17/14 09:55 Coumaphos mg/kg 0.011 U 0.017 11/17/14 09:55 Diazinon mg/kg 0.0032U 0.017 11/17/14 09:55 Dichlorvos mg/kg 0.0040U 0.017 11/17/14 09:55 Dimethoate mg/kg 0.0032U 0.017 11/17/14 09:55 Disulfoton mg/kg 0.0031U 0.017 11/17/14 09:55 Ethion mg/kg 0.0036U 0.017 11/17/14 09:55 Famphur mg/kg 0.0037U 0.017 11/17/14 09:55 Malathion mg/kg 0.0031U 0.017 11/17/1409:55 Methyl parathion mg/kg 0.0045U 0.017 11/17/14 09:55 Mevinphos mg/kg 0.0030U 0.017 11/17/14 09:55 Monocrotophos mg/kg 0.0072U 0.033 11/17/14 09:55 Parathion(Ethyl parathion) mg/kg 0.0065U 0.033 11/17/14 09:55 Phorate mg/kg 0.0058U 0.033 11/17/14 09:55 Phosmet mg/kg 0.0072U 0.017 11/17/14 09:55 4-Chloro3nitrobenzotrifluodde % 84 28.9-136.7 11/17/14 09:55 LABORATORY CONTROL SAMPLE: 1057381 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Atrazine mg/kg .2 0.25' 124 58-130 Azinphos,methyl(Guthion) mg/kg .067 0.077 115 47-143 Bromacil mg/kg .13 0.12 91 N2 Carbophenothion(Trithion) mg/kg .067 0.076 114 53-130 Chlorpyrifos mg/kg .067 0.070 105 60-130 Coumaphos mg/kg .067 0.073 109 50-130 Diazinon mg/kg .067 0.075 112 57-130 Dichlorvos mg/kg .067 0.064 96 51-153 Dimethoate mg/kg .067 0.086 130 42-144 Disulfoton mg/kg .067 0.073 109 57-130 Ethion mg/kg .067 0.065 98 57-130 Famphur mg/kg .067 0.080 120 59-132 Malathion mg/kg .067 0.076 113 47-160 Methyl parathion mg/kg .067 0.066 100 57-130 Mevinphos mg/kg .067 0.060 89 50-148 Monocrotophos mg/kg .13 0.15 111 41-133 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 15 of 25 i POOP,/ Pace Analytical Services,Inc. � 3610 Park Central Blvd N aceAnalytical Pompano Beach,FL 33064 (� www.pacelabs.com 954-582-4300 I. QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 LABORATORY CONTROL SAMPLE: 1057381 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Parathion(Ethyl parathion) mg/kg' ..13 0.14 107 54-130 Phorate mg/kg .13 0.14 103 48-130 Phosmet mg/kg .067 0.080 120 52-136 4-Chloro3nitrobenzotrifluoride % 79 28.9-136.7 I Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 16 of 25 Pace Analytical Services,Inc. Q rt / 3610 Park Central Blvd N alci AI!alXical( Pompano Beach,FL 33064 I www.pacelabs.com 954-582-4300 QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: OEXT/19689 Analysis Method: EPA 8151 QC Batch Method: EPA 8151 Analysis Description: 8151 GCS Herbicides Associated Lab Samples: 35163711001,35163711002 METHOD BLANK: 1057102 Matrix: Solid Associated Lab Samples: 35163711001,35163711002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 2,4,5-T mg/kg 0.0011U 0.0063 11/14/1417:28 2,4,5-TP(Silvex) mg/kg 0.00079U 0.0063 11/14/14 17:28 2,4-D mg/kg 0.0075U 0.031 11/14/1417:28 2,4-DB mg/kg 0.017U 0.063 11/14/1417:28 Bentazon mg/kg 0.0019U 0.0031 11/14/1417:28 Dalapon mg/kg 0.0061 U 0.030 11/14/14 17:28 Dicamba mg/kg 0.0013U 0.0031 11/14/1417:28 Dinoseb mg/kg 0.0015U 0.0063 11/14/1417:28 Pentachlorophenol mg/kg 0.00080U 0.00094 11/14/1417:28 Picloram mg/kg 0.00053U 0.0031 11/14/1417:28 2,4-DCAA(S) % 100 66-130 11/14/14 17:28 LABORATORY CONTROL SAMPLE: 1057103 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 2,4,5-T mg/kg .04 0.021 52 46-137 2,4,5-TP(Silvex) mg/kg .04 0.047 118 63-133 2,4-D mg/kg .2 0.20 100 40-137 2,4-DB mg/kg .4 0.47 118 70-130 Bentazon mg/kg .02 0.014 70 58-130 Dalapon mg/kg .2 0.17 83 17-137 Dicamba mg/kg .02 0.017 88 43-130 Dinoseb mg/kg .04 0.0072 18 10-177 Pentachlorophenol mg/kg .006 0.0071 119 70-144 Picloram mg/kg .02 0.023 116 10-147 2,4-DCAA(S) %. 99 66-130 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1057147 1057148 MS MSD 35163711001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual 2,4,5-T mg/kg 0.0013U .047 .047 0.026 0.026 55 55 46-137 .4 40 2,4,5-TP(Silvex) mg/kg 0.00094U .047 .047 0.055 0.050 116 106 63-133 9 40 2. mg/kg 4-D m /k 0.0089U .24 .24 0.22 0.21 94 90 40-137 4 40 2,4-DB mg/kg 0.020U .47 .47 0.50 0.50 105 107 70-130 1 40 Bentazon mg/kg 0.0023U .024 .024 0.027 0.026 115 111 58-130 4 40 Dalapon mg/kg 0.0072U .24 .24 0.092 0.081 39 34 17-137 13 40 Dicamba mg/kg 0.0015U .024 .024 0.016 0.015 69 62 43-130 11 40 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 17 of 25 Pace Analytical Services,Inc. _ aceAnal Kcal 3610 Park Central Blvd N t_. Pompano Beach,FL 33064 www.pacelabs.cam 954-582-4300 I QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1057147 1057148 MS MSD 35163711001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qua[ Dinoseb mg/kg 0.0018U .047 .047 0.00611 0.00741 13 16 10-177 40 Pentachlorophenol mg/kg 0.0015 .0071 .0071 0.0073 0.0087 83 103 70-144 17 40 Picloram mg/kg 0.000631.1 .024 .024 0.015 0.017 64 70 10-147 10 40 2,4-DCAA(S) % 94 91 66-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 18 of 25 Pace Analytical Services,Inc. 3610 Park Central Blvd N aceAnalytical Pompano Beach,FL 33064 www.paWabs.wm 954-582-4300 QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: OEXT/19683 Analysis Method: FL-PRO QC Batch Method: EPA 3546 Analysis Description: FL-PRO Soil Associated Lab Samples: 35163711001 METHOD BLANK: 1056611 Matrix: Solid Associated Lab Samples: 35163711001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Petroleum Range Organics mg/kg 2.51-1 4.0 11/14/14 08:02 N-Pentatriacontane(S) % 105 42-159' 11/14/1408:02 o-Terphenyl(S) % 110 62-109 11/14/14 08:02 S3 LABORATORY CONTROL SAMPLE: 1056612 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Petroleum Range Organics mg/kg 200 209 104 63-153 N-Pentatriacontane(S) % 110 42-159 o-Terphenyl(S) % 110 62-109 S7 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1056858 1056859 MS MSD 35163467002 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %°Rec Limits RPD RPD Qual Petroleum Range Organics mg/kg 2.5U 199 200 204 200 102 100 63-153 2 20 N-Pentatriacontane(S) % 106 110 42-159 o-Terphenyl(S) % 110 109 62-109 S7 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 19 of 25 Pace Analytical Services,Inc. 3610 Park Central Blvd N ace Analy dal Pompano Beach,FL 33064 www pacelabs.com 954-582-4300 i. QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: OEXT/19694 Analysis Method: FL-PRO QC Batch Method: EPA 3546 Analysis Description: FL-PRO Soil Associated Lab Samples: 35163711002 METHOD BLANK: 1057407 Matrix: Solid Associated Lab Samples: 35163711002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Petroleum Range Organics mg/kg 2.5U 4.0 11/15/14 09:37 N-Pentatriacontane(S) % 96 42-159 11/15/14 09:37 o-Terphenyl(S) % 97 62-109 11/15/14 09:37 LABORATORY CONTROL SAMPLE: 1057408 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Petroleum Range Organics mg/kg 197 210 107 63 7153 N-Pentatriacontane(S) % 99 42-159 o-Terphenyl(S) % 100 62-109 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 20 of 25 Pace Analytical Services,Inc. �CGA nn� 3610 Park Central Blvd N VG HI Ia' l I,V l Pompano Beach,FL 33064 wwwpacetabs.com 954-582-4300 QUALITY CONTROL DATA Project: SAXONY WEST Pace Project No.: 35163711 QC Batch: PMST/2947 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 35163711001,35163711002 SAMPLE DUPLICATE: 1058845 35163711001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 15.4 12.9 18 10 J(D6) SAMPLE DUPLICATE: 1058846 35163908009 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 5.7 5.1 12 10 J(D6) Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 21 of 25 Pace Analytical Services,Inc. '� 3610 Park Central Blvd N . Pompano Beach,FL 33064 www pacelabs.com 954-582-4300 s QUALIFIERS Project: SAXONY WEST Pace Project No.: 35163711 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to changes in sample preparation,dilution of the sample aliquot,or moisture content. ND-Not Detected at or above adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit. S-Surrogate 1,2-Diphenylhydrazine(8270 listed analyte)decomposes to Azobenzene. Consistent with.EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. LABORATORIES PASI-O Pace Analytical Services-Ormond Beach ANALYTE QUALIFIERS I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J(D6) Estimated Value.The relative percent difference(RPD)between the sample and sample duplicate exceeded laboratory control limits. J(LO) Estimated Value.Analyte recovery in the laboratory control sample(LCS)was outside QC limits. J(MO) Estimated Value.Matrix spike recovery was outside laboratory control limits. J(M1) Estimated Value.Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS) recovery. J(R1) Estimated Value.RPD value was outside control limits. L3 Analyte recovery in the laboratory control sample(LCS)exceeded QC limits.Analyte presence below reporting limits in associated samples. Results unaffected by high bias. N2 The lab does not hold TNI accreditation for this parameter. S3 Surrogate recovery exceeded laboratory control limits.Analyte presence below reporting limits in associated samples. Results unaffected by high bias. S7 Surrogate recovery outside control limits(not confirmed by re-analysis). REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 22 of 25 Pace Analytical Services,Inc. 3610 Park Central Blvd N aceAnalytical Pompano Beach,FL 33064 I www.pacelabs.com 954-582-4300 (QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: SAXONY WEST Pace Project No.: 35163711 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 35163711001 B-1 S-10 EPA 3546 . OEXT/19690 EPA 8081 GCSV/12935 35163711002 Stockpile Sample EPA 3546 OEXT/19690 EPA 8081 GCSV/12935 35163711001 B-1 S-10 EPA 3546 OEXT/19664 EPA 8141 GCSV/12921 35163711002 Stockpile Sample EPA 3546 OEXT/19692 EPA 8141 GCSV/12939 35163711001 B-1 S-10 EPA 8151 OEXT/19689 EPA 8151 GCSV/12931 35163711002 Stockpile Sample EPA 8151 OEXT/19689 EPA 8151 GCSV/12931 35163711001 B-1 S-10 EPA 3546 OEXT/19683 FL-PRO GCSV/12924 35163711002 Stockpile Sample EPA 3546 OEXT/19694 FL-PRO GCSV/12932 35163711001 B-1 S-10 EPA 3050 MPRP/21509 EPA 6010 1CP/13168 35163711002 Stockpile Sample EPA 3050 MPRP/21509 EPA 6010 ICP/13168 35163711001 B-1 S-10 EPA 7471 MERP/5098 EPA 7471 MERC/5091 35163711002 Stockpile Sample EPA 7471 MERP/5098 EPA 7471 MERC/5091 35163711001 B-1 S-10 ASTM D2974-87 PMST/2947 35163711002 Stockpile Sample ASTM D2974-87 PMST/2947 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, _ ... Date: 11/17/2014 04:50 PM without the written consent of Pace Analytical Services,Inc.. Page 23 of 25 f� v IIIIIIII E 8 0 u ii w�'m m�'o °m m o U ¢ i.� u Q o U �uNaaa� o'o'vo—m53 QZ .ON YN 0 S 4) W a-(L Cc— L I Q Q¢W :e .. tiEo pO a ti U 0 m c 1 L W aa.aN1F-O�U, I v 11 m P = m`� d'. U u E N ca @ S�ZZ ce. c rn r m %j o y Nov° � m rnd� • W LL U` 2 {' I LL � o v t U ' �m5.m ,m r '' m!Jp 10 a - C>>m�^c.AC o `4I V N �;C cc > u J JaC7 o mz 7 m '. a .<Em Q Z o rn o p mc9w¢3ocn� tm" �Mp2 f :c H o y $ m 9 U v ma oo :: Cp(np I :o Z o m 3 m E mEmEEE ) avm OZN c0 QUa¢V¢¢rn E p�LLLL ��J Z22Z -,a d m d a. U 3' » c7 S a N x U W W¢ p U ___t o m ° m o M 000U� 4 8 m a ¢Ua J¢Uad¢�Oarn w !z c� a w v > a 0609 pea- -ssl® Z I3ldWVX3 z J s -T 0 7: ;. d m ❑ ❑ ❑ El 10 ❑ ❑ ❑ ❑ 11 0 8 M WIN x ! .' 0 4s r r ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ > CL } ❑ ❑ ❑ ❑ ❑ ❑ ❑ ❑ <c, a C { c w q t 2 a v-y1 > O °� -- > r " a El El El ❑ ❑ ❑ .❑ ❑ W ` Q j= c ew Pd v IL Awn L a ('J S17 G 1 > p Z � :.1 n 1 Ya 2 o i = 1 4 J p a :�? ' a N a T ca M m _ �, z E >1 a ° a�E U. a W U) ... C/) t t V E. a c C.3 LO y _y v '•i p, s In�.. _ E ~ J Z CL ca cn r a) c r N (� d Cfl f` 00 O a } E ' o °v E( ° '8IclWES � N cep � �Of 25 _n U c a az cnU v: "E cument Name: Document Revised: 'Fo Sample Condition Upon Reo2jp-, m October 9,2013 Document No.: Issuing Au`onus: F-r—L-C-007 rev.05 Pace Florida Quality Offiar-e A OW 1M--Z ot Aft,Kok Client Name RY G Date* USPS Client Com ace Courier.C- 1 Fed EX C2 UPS mercial 'P Tracking# Custody Seal on Cooler/Box Present: yzs no Seals intact U—.--'yes V110 Date and I iti person examining Packing 11aterial: Bubble Wrap f--Bubble Baos None other. contents. Thermometer Used Type of Ice Blue None /(Temp should be above ireeZing In 6'C).ft blow O'G,then was CoolerTemperatturelc (Correction Factor) (Actual) s2mple frozen? Ely Receipt of samples siatislactory: JY— QNo Rush TAT requested on COC: PE I Iflyes,then all conditions belo",were met-- IF no,then mark box&describe*issue(use comments area if necessary): Chain of Custody Present ❑ Chain of Custody Filled Out ❑ relinquished Signature&Sampler Name CDC ❑ Samples Arrived within Hold Time El Sufficient Volume ❑ Correct Containers Used ❑ Containers Intact Sample Labels match CDC(sample IDs&date/time of collection) ❑ No Labels: No T-ime/Dale on Labels: All container needing presservaflbn are found to be in ❑ compliance with EP„reczrnmendabon. No Headspace in VOA Vials(>6mm): Client NotiflcationJ Resolution: Person Contacted: Dalarl-ime: Comments/Resolution(use back for additional comments): Protect MariaaeT Review: Date: Finished Product Information Only F.P.Sample ID: Size&Qty of Bottles Received Y, 5 Gat Production Code: x 2.5 Gat )c I Gat DateMme Opened: x I Liter x 500 r-.,L Number of Unopened Bottles Remaining: x 250 mL x Other: Extra Sample in Shed: yes No Page 25 of 25 Attachment- B Department of Regulatory and Economic Resources Environmental Resources Management MIAMI-DADE 701 NW 1st Court,4th Floor Miami,Florida 33136-3912 T 305-372-6700 F 305-372-6982 Carlos A. Gimenez, Mayor miamidade.gov February 19, 2015 CERTIFIED MAIL NO. 7013 2630 0001 2418 6941 RETURN RECEIPT REQUESTED Jimmy L Morales, City Manager City of Miami.Beach 1700 Convention Center Drive Miami Beach, FL 33139 Re: Soil Re-Use evaluation for soils from the Faena site at 34 Street and Collins Avenue and from the FDOT Alton Road Project between Michigan Avenue and Dade Blvd. and stored on the west side of the Par 3 Golf Course ( tracked under SW-1360 File-9507) located at, near, or in the vicinity of Praire Avenue and 28 Street, Miami Beach, Miami-Dade County, Florida. Dear Mr. Morales: The Department of Regulatory and Economic Resources-Division of Environmental Resources Management (DERM) has conducted site inspections and obtained soil samples from the above referenced soils currently being stored on the west side of the City of Miami beach Par 3 Golf course. The inspections and sampling were conducted by DERM based on a request for soil re-use initiated by the City of Miami Beach in an email dated January 23, 2015. Based on an Inspection conducted by DERM on February 5, 2015, several distinct groups of soil piles were noted including grey sand, organic peat mixed with marl, organic top soil, and mixed aggregate with organics. Significant portions of the various types of soil were also noted to be spread across the west side of the Par 3 golf course along with a western berm of said material. Analytical soil samples for chemicals of concern ranging from VOCs, TRPH, PAHs, Metals, TOC, and Chloride were obtained from representative locations within the distinct soil piles. The following comments are provided based on the DERM inspection and sample results: 1. Solid waste consisting of brick, tiles, PVC, plastic, rebar, metal and other various material were noted in several soil piles and graded areas. Based on an initial screening, the solid waste impacted material was noted primarily in the southern half of the soil stock pile area as depicted on the attached map. Be advised that all soil piles and distributed/graded material that contains solid waste shall be removed and properly disposed. In the event that the City of Miami Beach elects to separate the solid waste material for potential re-use of the remaining screened material, be advised that specific approval from the Department is required to re-use the recovered screened material (e.g. screening). You may submit a separate Corrective Action Plan (CAP) for review and approval of a one-time processing (i.e., mechanical screening) and appropriate disposal of solid waste. Please contact Rashid Istambouli, P.E., of DERMs' Pollution Regulation Division for further information. 2. Regardless of the presence of solid waste, all top soil either stored in piles or distributed/graded across the site shall require removal and proper disposal. Arsenic levels up to 19 mg/kg and exceeding the barrier islands background level of 5.2 mg/kg were identified in multiple soil piles. Therefore, screening and removal of solid waste is not an option and disposal of the entire piles representing this material shall be properly disposed. The locations of these piles were noted in the southern portion of the site. a f J i Mr. Morales SW-1360/File-9507 February 19, 2015 Page 2 3. Regardless of the presence of solid waste, the soil piles located on the northern end of the site as depicted in the attached map require removal and proper disposal based on the presence of strong petroleum odors which constitute a nuisance condition in accordance with Chapter 24, Code of Miami-Dade County. 4. Please note that per the February 2, 2015 DERM email and based on existing information at that time, a minimum of 6 representative samples from the Faena sand were required per the soil re- use guidance. However, subsequent to this email and as observed during the February 5, 2015 DERM inspection, the Faena sand has been distributed and graded throughout the western portion of the PAR 3 golf course, including mixing with other material present at the site. Based on the above and as part of the required CAP, a soil sampling plan to include installing representative soil borings through the distribution area of the Faena sand is required. The plan shall clearly identify on a scaled map the distribution area and depth of the Faena sand. 5. Be advised that a follow-up inspection conducted by DERM on February 18, 2015 identified that additional material of unknown origin has been deposited and is being stored at the subject site. Reference additional piles located immediately to the west of the soil piles with petroleum odors. The origin of this material shall be provided and a plan for appropriately characterizing this material shall also be included in the CAP. Based on the above, within thirty (30) days upon receipt of this letter submit a CAP addressing the above comments. Be advised that the CAP shall contain a site map clearly depicting the areas intended for removal and disposal based on the material composition described above. Upon receipt, DERM will schedule a site visit to confirm the data submitted in the CAP. Be advised that the referenced soils shall not be removed, relocated, or distributed across the site without DERM approval. Please also find attached the results of the February 5, 2015 DERM soil pile samples. DERM shall be notified in writing a minimum of three (3) working days prior to the implementation of any field activities. Email notifications shall be directed to DERMPCD @miamidade.gov. Please include the DERM file number on all correspondence. If you have any questions concerning the above, please contact Thomas Kux, P.G. (Kuxt @miamidade.gov) of the Environmental Assessment Section at (305) 372-6700. Sincerely, Wilbur Mayorga, P.E., Chief Environmental Monitoring & Restoration Division TK attach ec: Lee Hefty, Mayra Flagler, Rashid Istambouli P.E., Johnny Vega P.E., DERM Margarita Wells, City of Miami Beach, MargaritaWells(cDmiamibeachfl.gov Betsy Wheaton, City of Miami Beach, ewheaton(aDmiamibeachfl.gov Bruce Mowry, City of Miami Beach, BruceMowry(aD-miamibeachfl.gov w.& pt ...... .. .......... CL no CU E 4-J m �' y� Vim! mgrcy:. �L -:. a 0 E m to 4-J ra 4-J .................... 4i 7 4-J U CL E cn M V) cz w C 0 4-j CL 4� m V) 4-J Ln C JIF 0 CL Ln CO 0 - 4-1 > (3) LL a. co Uj .11 rl 75 "77 LU